This dissertation presents a Nuclear Magnetic Resonance (NMR) study of anisotropic superconductors, MgB$_2$ and Bi$_2$Sr$_2$CaCu$_2$O$_{8+\delta}$ (Bi2212), and diffusion in glass-forming aqueous solutions of glycerol. In glycerol and deuterated water mixtures, the diffusion of glycerol is measured selectively by the $^1$H NMR stimulated echo technique in the gradient field of a...